BRYN MAWR COLLEGE
Organic Chemistry Laboratory
Chemistry 212
Schedule for Semester II, Summer 2013
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Dates Lab Procedure Experiment Title Experiment Type
7/08 Diels-Alder (DOCX)
Diels-Alder (PDF)

Diels-Alder Reaction/Set-up/Check-in

F, P
7/10



Diels-Alder Reaction/Recrystallizaton Oxidation of Camphor
General Lab Information

7/15

Kinetically Controlled Friedel Crafts Reaction

Thermodynamically Controlled Friedel Crafts


O, G
7/17 Stereoselective Reduction of Ethyl Acetoacetate (DOCX)
Stereoselective Reduction of Ethyl Acetoacetate (PDF)

Conferences/Make up
Enzymatic Reduction of Ethyl acetoacetate
Start Reaction

 
7/22 Stereoselective Reduction of Ethyl Acetoacetate (DOCX)
Stereoselective Reduction of Ethyl Acetoacetate (PDF)

Enzymatic Reduction of Ethyl acetoacetate

7/24 Synthesis of Flutamide (PDF)
Synthesis of Flutamide (DOCX)
Microscale Synthesis of Flutamide
* Aldol synthesis of an alpha, beta unsaturated ketone

P
7/29 Synthesis of Warfarin (PDF)

* A Green, Efficient, Enantioselective Synthesis of Warfarin and Warfarin analogues

P
8/01 Synthesis of Warfarin * Purification and Analysis of Warfarin and analogues
8/07 Purification and Analysis of Warfarin and analogues
Total Synthesis Project
see assignments

G, Literature style paper and assignments


P Preparative experiment/write-up/conference
F Form write-up
G Group experiment/write-up.  Only one report per group.
L Literature Style Paper will be written
O Conference - group meets with instructor, no write up
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